PTQ Q4 2023 Issue

Overhead

Top reux

O - gas

1

Reux

9

Light naphtha

Feed

15

Top pumparound

21

100%

65%

45

LV

Heavy naphtha side str i pper

0%

46

Side reboiler

47 48

49

Bottom reboiler

Kerosene side stripper

Kerosene pumparound

Bottom

Figure 5 Operational moves for process optimisation

Figure 6 DeIsoButaniser (DIB) configuration

Scrutinising the heavy naphtha draw circuit revealed another root cause. The heavy naphtha draw circuit geom- etries and pressure measurement values are summarised in Figure 4 . The hydraulic balance was constructed based on the draw geometries and measured pressure values. The simplified hydraulic balance is also illustrated in Figure 4. Heavy naphtha flow to the side stripper was controlled by the side stripper level. The static inlet pressure of the level control valve was 35 psig. If the upper draw was full, pressure at the upper draw location would be 10 psi higher. A static pressure of 45 psig was ample to maintain driving force. Meanwhile, measured pressure at the heavy naphtha lower draw was not matched to possible head pressure at the tie-in point unless the upper draw was completely empty. In this hydraulic balance, the lower draw would be pushed back into the crude atmospheric tower by the upper draw liquid. This undesired reverse flow caused seven underloaded fractionation trays and downgraded fractionation performance. Liquid from the heavy naphtha upper draw bypassed seven fractionating trays. It resulted in low tray efficiency. Kerosene pumparound instability was also reviewed. The kerosene pumparound configuration was previ - ously depicted in Figure 1. Three different draw nozzles were available. Operators thought a single nozzle was not large enough to draw both product and pumparound streams. Kerosene product and pumparound streams

were withdrawn at different trays. The configuration was also believed to maximise fractionation between kerosene and diesel. A detailed tower internal evaluation revealed that sub- cooled pumparound liquid could be continuously sucked into the kerosene product draw nozzle. This undesired flow behaviour caused less pumparound return liquid, con - tributing to heat transfer. Pumparound heat removal could be reduced by less condensation. 1 Reduced pumparound flow due to recent circuit fouling exaggerated pumparound instability. Case study 1: Optimisation solutions Operational moves illustrated in Figure 5 were imple- mented to prevent the heavy naphtha reverse flow and

Crude atmospheric tower performance

Operating parameter

Pre-optimisation Post-optimisation

Crude charge, b/d

Base Base Base Base

Base

Heavy naphtha yield, b/d

+ ∆ 5%

Kerosene yield, b/d

Base

Kerosene flash point, ºF Gap (kerosene T10- heavy naphtha T90), ºF

+ ∆ 2ºF

Base

+ ∆ 5ºF

Heavy naphtha tail (EP-T90), ºF

Base

- ∆ 15ºF

Table 1

91

PTQ Q4 2023

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